CHEM 232 Experimental Organic Chemistry I
Course prerequisites: Successful completion of, or concurrent enrollment in Organic Chemistry I.
Required course materials:
1. Bound lab notebook with duplicate pages (from previous course, if available).
2. Safety glasses
3. Copy of Experimental Organic I lab manual
Course requirements/grading points: 1. Succesful completion of
all labs
and lab write-ups
50
2. Three 50 point quizzes
150
3. technique evaluation
50
Lab Schedule
Week Activity______________________________________________________________
1. Check-in/safety
discussion/lab orientation
2. Recrystallization
of Benzoic acid and melting points
3. Distillation of
a binary mixture
4. Capillary GC analysis
of the distillation fractions
5. Extraction of Caffeine
from tea
6. HPLC analysis of
caffeine
7. (Quiz at beginning
of lab)
Bromination of trans-cinnamic acid
8. Thin layer chromatography
9. Flash chromatography
with synthesis of benzyl acetate and HNMKR analysis of product
10. Cont.
11. Synthesis of cyclohexene
with FTIR product analysis
12. ( Quiz
2)
Synthesis of benzyl alcohol with FTIR, HNMR, and GC-MS product analysis
13. cont.
14. cont.
15. Introduction to
Molecular Modeling
16. Last quiz
and check-out